Browsing by Author "Emetere, Moses E."

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    Industrial- and automotive-used lubricating oils recycling cum acidic sludge treatment
    (Springer, 2019) Oladimeji, Temitayo E; Oguntuashe, Kehinde M.; Emetere, Moses E.; Efeovbokhan, Vincent E.; Odunlami, Olayemi A.; Obanla, Oyinlola R.
    Increased rise of industries and car usage in Nigeria and urban development is exponentially on the increase giving rise to multiple waste generation. Evaluation of the different recycling processes showed that acid-clay process has the highest environmental risk as well as the lowest cost; hence, this work added a treatment method for the slurry produced after treatment with acid-clay method, thereby reducing the environmental concern caused by acid and acid sludge formed in the process. The acid ratio was varied between 0 and 20% and adsorbent ratio between 15 and 25%. Automotive-used lubricating oil and industrial-used lubricating oil were treated using two different samples, acid and adsorbent. An increase in acid concentration showed a significant difference over the properties of oil such as density, viscosity, flash point, and other physiochemical properties nevertheless increasing the amount of acid over the optimum point made on significant change. Varying of adsorbent ratio showed little significant effect to density and flash point, while yield and viscosity were unaffected. Optimum point being at 10% acid and 25% adsorbent gave optimal result. All metal contaminants are substantially removed; total base number was improved, while increase in flash point suggested the method effectiveness. Treatment of used industrial oil was found to be easier to re-refine due to less contamination.
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    Production of activated carbon from sawdust and its efficiency in the treatment of sewage water
    (Materials Science Forum, 2025) Oladimeji, Temitayo E; Olaniyan, Ifeoluwa F.; Emetere, Moses E.; Adeoye, John B.; Odunlami, Olayemi, A.; Abatan, Olubunmi G.
    The use of activated carbon for wastewater treatment has been established based on sustainability and cost. This study delves into the intricate process of producing activated carbon from cow and goat bones and explores the efficiency of this material in removing contaminants from distillery wastewater. The samples were carbonized at 700°C in a muffle furnace, then crushed in a mortar after cooling. The crushed samples were activated using 0.4M phosphoric acid for 24 hours and washed with distilled water, and finally oven dried. The elemental and microstructural was carried on the prepared activated carbon (AC) samples using X-ray Fluorescence (XRF) and Scanning Electron Microscopy (SEM). The heavy metals in the treated water were tested using Atomic Absorption Spectroscopy (AAS). The AC was used to treat waste water and factors on which adsorption depend, such as contact time (35 minutes and 60 minutes), adsorbent dosage (2.5g and 5g), and initial contaminant concentration (100% and 50%) were varied for each activated carbon sample (cow bone AC, goat bone AC, and a mixture of equal ratios of both). It was reported that activated carbon prepared from animal bones is rich in calcium. Also, chemical activation with phosphoric acid led to an increase in the external surface area of the particles with irregular cavities and pores. AC prepared from the mixture of cow and goat bones was most effective for distillery wastewater purification.